{"id":155264,"date":"2020-09-01T10:26:21","date_gmt":"2020-09-01T10:26:21","guid":{"rendered":"http:\/\/blog.hannaservice.eu\/regles-de-titrage-analyse\/"},"modified":"2022-10-10T11:58:08","modified_gmt":"2022-10-10T11:58:08","slug":"regles-de-titrage-analyse","status":"publish","type":"post","link":"https:\/\/blog.hannaservice.eu\/fr\/regles-de-titrage-analyse\/","title":{"rendered":"R\u00e8gles de titrage \u2013 Analyse"},"content":{"rendered":"\t\t
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Une analyse pr\u00e9cise \u00e9quivaut \u00e0 des r\u00e9sultats de premier ordre.<\/h2>\n

Une bonne pr\u00e9paration avant votre analyse aidera \u00e0 garantir que vos tests se d\u00e9roulent de mani\u00e8re fluide et pr\u00e9cise. Des pr\u00e9cautions doivent \u00e9galement \u00eatre prises apr\u00e8s l\u2019analyse pour vous assurer que votre \u00e9quipement fonctionne de mani\u00e8re optimale \u00e0 l\u2019avenir. Prendre cinq minutes suppl\u00e9mentaires pour mettre en point vos i et croiser vos t peut faire une diff\u00e9rence.<\/p>\n

Une analyse<\/h2>\n

# 5 Inspectez l\u2019instrumentation avant et apr\u00e8s l\u2019analyse<\/h3>\n

Afin de s\u2019assurer que les r\u00e9sultats du titrateur sont exacts, l\u2019instrument et l\u2019\u00e9lectrode doivent \u00eatre inspect\u00e9s avant et apr\u00e8s l\u2019analyse.<\/p>\n

Pr\u00e9-analyse<\/h4>\n

ELECTRODE<\/strong>:<\/h5>\n

L\u2019\u00e9lectrode est la partie du syst\u00e8me de titrage qui est charg\u00e9e de surveiller la r\u00e9action de titrage; il est essentiel de s\u2019assurer que l\u2019\u00e9lectrode continue de fonctionner comme pr\u00e9vu. La premi\u00e8re chose \u00e0 v\u00e9rifier est le niveau de remplissage de l\u2019\u00e9lectrolyte. Cela devrait \u00eatre compl\u00e9t\u00e9 avec la solution appropri\u00e9e quand il tombe en dessous d\u2019un pouce du trou de remplissage. Il est \u00e9galement important que le bouchon de remplissage soit desserr\u00e9 ou enlev\u00e9 pendant le titrage pour permettre l\u2019\u00e9coulement r\u00e9gulier de l\u2019\u00e9lectrolyte dans l\u2019\u00e9chantillon qui est n\u00e9cessaire pour la stabilit\u00e9 de l\u2019\u00e9lectrode. V\u00e9rifiez toujours que l\u2019\u00e9lectrode a \u00e9t\u00e9 stock\u00e9e correctement avant l\u2019analyse. Pour des conditions de stockage appropri\u00e9es, reportez-vous au manuel de l\u2019\u00e9lectrode ou contactez votre repr\u00e9sentant commercial. Avant le d\u00e9but de l\u2019analyse, la pointe de l\u2019\u00e9lectrode doit \u00eatre rinc\u00e9e \u00e0 l\u2019eau d\u00e9min\u00e9ralis\u00e9e et exempte de d\u00e9bris. Pendant l\u2019analyse, l\u2019\u00e9lectrode doit \u00eatre immerg\u00e9e \u00e0 la profondeur appropri\u00e9e. Certaines \u00e9lectrodes n\u00e9cessiteront un \u00e9talonnage avant l\u2019ex\u00e9cution r\u00e9elle de votre titrage.<\/p>\n

Si vous n\u2019\u00eates pas s\u00fbr, n\u2019h\u00e9sitez pas \u00e0\u00a0contacter un repr\u00e9sentant Hanna.<\/a><\/p>\n

TITRANT:<\/strong><\/h5>\n

Avant l\u2019analyse de l\u2019\u00e9chantillon, assurez-vous que le flacon de titrant contient suffisamment de titrant et que le tube de distribution est fermement ins\u00e9r\u00e9 dans le titrant liquide. Il est \u00e9galement important de v\u00e9rifier la pr\u00e9sence de bulles d\u2019air dans la burette et le tube. Amorcer votre tubulure pour se d\u00e9barrasser des bulles est parfois n\u00e9cessaire. Une simple pointe de rin\u00e7age (une petite quantit\u00e9 de titrant est lib\u00e9r\u00e9e \u00e0 travers le tube de distribution) peut suffire \u00e0 dissiper les bulles d\u2019air pr\u00e8s de la pointe de distribution.<\/p>\n

\"\"<\/p>\n

N\u2019oubliez pas que le volume de titrant consomm\u00e9 pour atteindre un point final est directement pris en compte dans les r\u00e9sultats.<\/p>\n

Astuce HANNA:<\/strong>\u00a0Rien n\u2019est pire que d\u2019avoir une courbe de titrage parfaite, puis de constater que de l\u2019air a \u00e9t\u00e9 aspir\u00e9 de la bouteille de titrant en raison d\u2019un titrant insuffisant (prenez-le de nous!). V\u00e9rifiez toujours votre niveau de titrant.<\/span><\/p><\/blockquote>\n

\n
Contactez un expert en titrage Hanna Instruments d\u00e8s maintenant!<\/a><\/div>\n

Analyse post\u00e9rieure<\/h4>\n

Imm\u00e9diatement apr\u00e8s la fin du titrage, l\u2019\u00e9lectrode doit \u00eatre retir\u00e9e de l\u2019\u00e9chantillon. Une exposition prolong\u00e9e \u00e0 l\u2019\u00e9chantillon peut endommager les \u00e9lectrodes et raccourcir leur dur\u00e9e de vie ainsi qu\u2019affecter la r\u00e9ponse des \u00e9lectrodes, le bruit des \u00e9lectrodes et affecter les \u00e9chantillons suivants.<\/p>\n

Pour \u00e9viter toute contamination crois\u00e9e, il est important que l\u2019\u00e9lectrode, l\u2019h\u00e9lice de l\u2019agitateur, le capteur de temp\u00e9rature (le cas \u00e9ch\u00e9ant) et la pointe de dosage soient rinc\u00e9s avec de l\u2019eau d\u00e9sionis\u00e9e entre les \u00e9chantillons et une fois la charge de travail termin\u00e9e. Si vous travaillez avec des \u00e9chantillons qui pourraient obstruer ou s\u2019accrocher aux \u00e9lectrodes, il existe des solutions de nettoyage sp\u00e9ciales et des instructions pour vous garder en pleine forme.<\/p>\n

Lors du stockage des syst\u00e8mes pendant de longues p\u00e9riodes, le bouchon de remplissage d\u2019\u00e9lectrode doit \u00eatre resserr\u00e9 ou remplac\u00e9 pour \u00e9viter l\u2019\u00e9vaporation de la solution de remplissage d\u2019\u00e9lectrolyte.<\/p>\n<\/div>\n\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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Restez \u00e0 l\u2019\u00e9coute pour la partie 3 \u2013 Examen des r\u00e9sultats!<\/h3>\n

Avez-vous manqu\u00e9 la partie 1? Pas de soucis, juste\u00a0cliquez ici<\/a>.<\/p>\n\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t<\/div>\n\t\t","protected":false},"excerpt":{"rendered":"

Une analyse pr\u00e9cise \u00e9quivaut \u00e0 des r\u00e9sultats de premier ordre. Une bonne pr\u00e9paration avant votre […]<\/p>\n","protected":false},"author":14,"featured_media":152770,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"site-sidebar-layout":"default","site-content-layout":"default","ast-site-content-layout":"default","site-content-style":"default","site-sidebar-style":"default","ast-global-header-display":"","ast-banner-title-visibility":"","ast-main-header-display":"","ast-hfb-above-header-display":"","ast-hfb-below-header-display":"","ast-hfb-mobile-header-display":"","site-post-title":"","ast-breadcrumbs-content":"","ast-featured-img":"","footer-sml-layout":"","ast-disable-related-posts":"","theme-transparent-header-meta":"default","adv-header-id-meta":"","stick-header-meta":"","header-above-stick-meta":"","header-main-stick-meta":"","header-below-stick-meta":"","astra-migrate-meta-layouts":"default","ast-page-background-enabled":"default","ast-page-background-meta":{"desktop":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"tablet":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"mobile":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""}},"ast-content-background-meta":{"desktop":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"tablet":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"mobile":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""}},"footnotes":""},"categories":[354,398],"tags":[],"class_list":["post-155264","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-industry","category-laboratoire"],"yoast_head":"\nR\u00e8gles de titrage \u2013 Analyse - Hanna Instruments Maroc<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/blog.hannaservice.eu\/fr\/regles-de-titrage-analyse\/\" \/>\n<meta property=\"og:locale\" content=\"fr_FR\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"R\u00e8gles de titrage \u2013 Analyse - Hanna Instruments Maroc\" \/>\n<meta property=\"og:description\" content=\"Une analyse pr\u00e9cise \u00e9quivaut \u00e0 des r\u00e9sultats de premier ordre. 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