{"id":154939,"date":"2020-09-01T10:26:21","date_gmt":"2020-09-01T10:26:21","guid":{"rendered":"http:\/\/blog.hannaservice.eu\/pravila-titracije-analiza\/"},"modified":"2022-10-07T13:12:25","modified_gmt":"2022-10-07T13:12:25","slug":"pravila-titracije-analiza","status":"publish","type":"post","link":"https:\/\/blog.hannaservice.eu\/hr\/pravila-titracije-analiza\/","title":{"rendered":"Pravila titracije \u2013 analiza"},"content":{"rendered":"\t\t
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Precizna analiza garantira vrhunske rezultate!<\/h2>\n

Pravilna priprema prije analize pomoc\u0301i c\u0301e vam da testovi koje obavljate pro\u0111u glatko i bez smetnji. Tako\u0111er treba voditi ra\u010duna o post-analizi kako biste bili sigurni da va\u0161a oprema u buduc\u0301nosti radi optimalno. Ostavite dodatnih pet minuta svog vremena kako biste provjerili da li ste sve \u010dinjenice uzeli u obzir.<\/p>\n

Analiza<\/h2>\n

#5 Provjerite opremu prije nego \u0161to zapo\u010dnete analizu<\/h3>\n

Da biste bili sigurni da su rezultati titratora to\u010dni, instrument i elektrodu treba pregledati prije i poslije analize.<\/p>\n

Pred-Analiza<\/h4>\n

ELEKTRODA<\/strong>:<\/h5>\n

Elektroda je dio sustava za titraciju koji je odgovoran za nadgledanje reakcije titracije; presudno je osigurati da elektroda i dalje funkcionira kako je predvi\u0111eno. Prva stvar koju treba provjeriti je nivo elektrolita. Koristite odgovaraju\u0107u elektrolitsku otopinu kada njegov nivo padne na oko 1 cm od otvora za punjenje. Tako\u0111er je va\u017eno da se poklopac za punjenje olabavi ili ukloni tokom titracije kako bi se omoguc\u0301io stalan protok elektrolita u uzorku koji je potreban za stabilnost elektroda. Uvijek provjerite da li je elektroda pravilno uskladi\u0161tena\/\u010duvana prije analize. Za pravilne uvijete skladi\u0161tenja pogledajte priru\u010dnik za elektrode ili kontaktirajte tehni\u010dko \u2013 prodajnog predstavnika HANNA Instruments. Prije po\u010detka analize, vrh elektrode treba isprati deioniziranom vodom i osloboditi se otpadaka. Tijekom analize, elektroda treba biti uronjena na odgovarajuc\u0301u dubinu. Neke elektrode c\u0301e zahtijevati kalibraciju prije stvarnog pokretanja titracije.<\/p>\n

Za sve eventualne nejasno\u0107e\u00a0kontaktirajte HANNA Instruments<\/a><\/p>\n

TITRANT:<\/strong><\/h5>\n

Prije analize uzoraka, uvjerite se da bo\u010dica sa titrantom sadr\u017ei dovoljno titranta i da je cijev\u010dica \u010dvrsto postavljena u teku\u0107i titrant. Tako\u0111er je va\u017eno provjeriti da li postoje zaostali mehuric\u0301i zraka u bireti i cijev\u010dicama. Ponekad je potrebno pripremiti cijev\u010dice da biste se rije\u0161ili mjehuric\u0301a. Jednostavno ispiranje vrha (mala koli\u010dina titranta se osloba\u0111a kroz cijev\u010dicu) mo\u017ee biti dovoljna da se razbiju svi mjehuric\u0301i zraka u blizini vrha.<\/p>\n

\"HI931_HI932<\/p>\n

Imajte na umu da se koli\u010dina titranta potro\u0161ena za postizanje krajnje to\u010dke direktno uzima u obzir u rezultatima.<\/p>\n

Hanna Savjet:<\/strong>\u00a0Nema ni\u0161ta gore nego kad dobijete savr\u0161enu krivulju titracije, a zatim se \u0161okirate uvidjev\u0161i da je zrak iz titrant boce usisan zbog nedovoljne koli\u010dine titranta (znamo kako je to!). Uvijek provjerite nivo titranta!<\/p><\/blockquote>\n

Kontaktirajte HANNA stru\u010dnjaka za titratore!<\/a><\/div>\n

Post Analiza<\/h4>\n

Neposredno nakon zavr\u0161etka titracije, elektrodu treba izvaditi iz uzorka. Dugotrajno izlaganje uzorku mo\u017ee prouzrokovati o\u0161tec\u0301enja elektrode i skratiti joj \u017eivotni vijek, kao i utjecati na odziv elektrode, \u0161umove elektroda i utjecati na uzastopne uzorke.<\/p>\n

Da bi se sprije\u010dila unakrsna kontaminacija, va\u017eno je da se elektroda, propeler mje\u0161alice, temperaturni senzor (ako postoji) i dozirni vrh isperu deioniziranom vodom izme\u0111u uzoraka i po zavr\u0161etku operacija. Ako radite sa uzorcima koji bi mogli za\u010depiti elektrode, postoje posebno formulirane otopine za \u010di\u0161\u0107enje i upute namijenjene da Va\u0161u elektrodu dovedu u \u201ctip \u2013 top\u201d stanje.<\/p>\n

Kad skladi\u0161tite sustave du\u017ee vrijeme, poklopac za punjenje elektrode treba zategnuti ili zamijeniti kako bi se sprije\u010dilo isparavanje elektrolita za punjenje.<\/p>\n\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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Ostanite uz nas, slijedi 3.dio \u2013 Pregled rezultata titracije!<\/h3>\n

Propustili ste prvi dio serije blogova o titraciji? Bez brige, sav materijal se nalazi\u00a0ovdje<\/a>.<\/p>\n\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t<\/div>\n\t\t","protected":false},"excerpt":{"rendered":"

Precizna analiza garantira vrhunske rezultate! Pravilna priprema prije analize pomoc\u0301i c\u0301e vam da testovi koje […]<\/p>\n","protected":false},"author":14,"featured_media":152769,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"site-sidebar-layout":"default","site-content-layout":"default","ast-site-content-layout":"default","site-content-style":"default","site-sidebar-style":"default","ast-global-header-display":"","ast-banner-title-visibility":"","ast-main-header-display":"","ast-hfb-above-header-display":"","ast-hfb-below-header-display":"","ast-hfb-mobile-header-display":"","site-post-title":"","ast-breadcrumbs-content":"","ast-featured-img":"","footer-sml-layout":"","ast-disable-related-posts":"","theme-transparent-header-meta":"default","adv-header-id-meta":"","stick-header-meta":"","header-above-stick-meta":"","header-main-stick-meta":"","header-below-stick-meta":"","astra-migrate-meta-layouts":"default","ast-page-background-enabled":"default","ast-page-background-meta":{"desktop":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"tablet":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"mobile":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""}},"ast-content-background-meta":{"desktop":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"tablet":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"mobile":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""}},"footnotes":""},"categories":[354,387],"tags":[],"class_list":["post-154939","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-industry","category-laboratorij"],"yoast_head":"\nPravila titracije \u2013 analiza - Hanna Instruments Hrvatska<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/blog.hannaservice.eu\/hr\/pravila-titracije-analiza\/\" \/>\n<meta property=\"og:locale\" content=\"hr_HR\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Pravila titracije \u2013 analiza - Hanna Instruments Hrvatska\" \/>\n<meta property=\"og:description\" content=\"Precizna analiza garantira vrhunske rezultate! 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